Fig. 2 t shaking (min) D Ir(IV) D Rh(III) 1 35.30168 1.16393 5 -- 1.55893 15 35.72109 1.33011 30 35.36906 1.66142 60 30.71336 1.6365 D average Ir(IV) = 34.27630 D average Rh(III) = 1.47018